LC-MS analysis. The 21mer sample described in this application note, unless otherwise mentioned as HPLC purified, is referred to as Sample A. A stock solution of 1 mg/mL was prepared for two 21mer samples of different purity. This solution was diluted to ™ 100 µg/mL before LC-MS analysis. Forced degradation
Mass Spectrometry Vials. Our certified, low adsorption (LA), LC/MS vials and kits are designed to reduce surface activity while improving analytical quantitation. The QSertVial™ microsampling device contains a fused, 300 μL glass insert and is compatible with most autosamplers.
Thermo Separation Products AS3000 Autosampler The Thermo SpectraSYSTEM AS3000 Autosampler provides outstanding performance and maximum flexibility in an LC sample processing system. This autosampler offers 120-vial capacity, multiple injection modes, random vial access, re-use of calibration standards, and priority sampling. **COVER HINGE BROKEN Manufacture Specifications Vial Capacity: 120
Cayman Chemical. convenient, precise quantification of linoleic acid by GC- or LC-MS. It includes a 50 µg vial of linoleic acid-d4 and a precisely weighed vial of unlabeled linoleic acid, with the precise weight (2-4 mg) indicated on the vial. This unlabeled linoleic acid can be used to quantify the linoleic.
Finally, we recommend a LC-MS/MS-based quantification method with a dynamic range of 0.5-40 μg/L for the assessment of hepcidin-25 in human serum that uses TFA-based mobile phases and silanized glass vials. Graphical abstract Structure of hepcidin-25 (Protein Data Bank, PDB ID 2KEF).
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